Tailored synthesis in nanoparticle permanent magnets (NPPMs)

bar chart showing oxygen content of Sm2Fe17N3 powder before and after washing.
Oxygen content of Sm2Fe17N3 powder before and after washing.

CMI researchers from Ames National Laboratory conducted the activity for this highlight

Innovation    
Optimized the post-synthesis washing procedure of Sm2Fe17N3 powders crucial to enhancing magnetic properties of the dense magnets.

Achievement    
Achieved ~5X reduction in oxygen content for Sm2Fe17N3 powders.

Significance and Impact    
Synthesis of Sm2Fe17N3 via reduction-diffusion of Sm2O3 leads to the formation of CaO as side product. Removing CaO without introducing undesirable surface oxidation leads to degradation of magnetic performance during consolidation. New solvents and washing condition resulted in our lowest measured oxygen content yet and yield sustainable, scabble process.

Hub Target Addressed    
Increasing the speed of discovery and integration.

 

line chart showing magnetic properties of unwashed Sm2Fe17N3 powder compared to after washing with condition 9.
Magnetic properties of unwashed Sm2Fe17N3 powder compared to after washing with condition 9.